Re: washing mirrors

Stan Thomas (thomas@cosmic.physics.utah.edu)
Sun, 09 Apr 1995 11:51:10 -0600

>
>>I should note that our mirrors are NOT protected by either SiO or MgF. We
>>use Aluminum Oxide.
>
>Yep. Al2O3 is quite tough - but the layer is rather thin.
>
>You might have mentioned that, whatever a person does, to make sure that
>their solution is not alkaline. Alkakine solutions will attack the aluminum
>oxide lae layer.
>
>I have washed my mirror about a dozen times, and have seen no sign of
>deterioration - and, like your mirrors, has no protective overcoating.
>
>Bill
>
>

Bill, The naturally occuring oxide layer is only approximately 50 nm thick. I use an electrochemical method to increase the natural oxide to around 1000 nm. At this thickness the surface is quite durable. We use the mirrors to observe Nitrogen fuorescence in the near ultra-violet region 300 nm - 400 nm. I optimized the oxide thickness for 1/2 wave at 337.1 nm (N2 laser line). With this oxide thickness I get from 85% to 90% reflectivity at 337.1 nm.

You are quite right that alkaline solutions will attack the aluminum. In fact, I use an NaOH solution to strip off the old aluminum coating when I want to re-aluminize a mirror. A bare aluminum mirror will strip very quickly using sodium hydroxide but an Al2O3 protected mirror takes a bit more work. :)

--
Stan Thomas <thomas@cosmic.physics.utah.edu>